3-methyl-N'-(3-methylbenzoyl)benzohydrazide (non-preferred name)

Base Information

• Chemical Name: 3-methyl-N'-(3-methylbenzoyl)benzohydrazide (non-preferred name)
• CAS No.: 59646-36-5
• Molecular Formula: C16H16N2O2
• Molecular Weight: 268.315
• Mol file: 59646-36-5.mol

Synonyms:2-(3-methylbenzoyl)hydrazide;N,N'-Bis-(m-toluoyl)-hydrazin;1,2-di-m-toluoylhydrazine;Benzoic acid, 3-methyl-, 2-(3-methylbenzoyl)hydrazide;3-methyl-benzoic acid;N,N'-Di-m-toluoyl-hydrazin;N,N'-di-m-toluoyl-hydrazine;N.N'-Di-m-toluyl-hydrazin;HMS2575K06;N,N'-bis(m-methylbenzoyl)hydrazine;

Chemical Property of 3-methyl-N'-(3-methylbenzoyl)benzohydrazide (non-preferred name)

Chemical Property:

• Boiling Point: 530.5°Cat760mmHg
• Flash Point: 209.3°C
• PSA: 58.20000
• Density: 1.163g/cm³
• LogP: 3.16000

Purity/Quality:

99% ^*data from raw suppliers

3-methyl-N'-(3-methylbenzoyl)benzohydrazide(non-preferredname) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methyl-N'-(3-methylbenzoyl)benzohydrazide (non-preferred name)

There total 7 articles about 3-methyl-N'-(3-methylbenzoyl)benzohydrazide (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-methylbenzoyl hydrazine (13050-47-0) → N'-(3′-methylbenzoyl)-3-methylbenzohydrazide (59646-36-5)

Guidance literature:

With sodium perborate; In acetic acid; Ambient temperature;

DOI:10.1002/jccs.199800126

Reference yield: 65.07%

C17H18N4O3 (202273-27-6) → N'-(3′-methylbenzoyl)-3-methylbenzohydrazide (59646-36-5)

Guidance literature:

With aluminium trichloride; at 170 - 180 ℃; for 3h;

Reference yield: 61.0%

3-Methylbenzoyl chloride (1711-06-4) → N'-(3′-methylbenzoyl)-3-methylbenzohydrazide (59646-36-5)

Guidance literature:

With sodium carbonate; hydrazine hydrate; In ethanol; at 0 ℃;

upstream raw materials:

3-methylbenzoyl hydrazine

3-Methylbenzoyl chloride

C₁₇H₁₈N₄O₃

Downstream raw materials:

2,5-bis(3-methylphenyl)-1,3,4-oxadiazole

2,5-di(m-tolyl)-1,3,4-thiadiazole

3,3'-(1,3,4-thiadiazole-2,5-diyl)dibenzoic acid

diethyl 3,3'-(1,3,4-oxadiazole-2,5-diyl)dibenzoate

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