1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride

Base Information

• Chemical Name: 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride
• CAS No.: 72155-37-4
• Molecular Formula: C₄₁H₃₆Cl₂N₂O₉
• Molecular Weight: 771.651

Synonyms:1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride

Chemical Property of 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride

Chemical Property:

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Technology Process of 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride

There total 2 articles about 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

[1-(4-Chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]-acetic acid 3-{2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]-acetoxy}-2-oxo-propyl ester (72155-38-5) → 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride (72155-37-4)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; water; benzene; for 1h; Ambient temperature;

DOI:10.1021/jm00175a003

Reference yield:

1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indole-3-acetyl chloride (20357-37-3) → 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride (72155-37-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 44 percent / pyridine / CH₂Cl₂ / 17 h / Ambient temperature

2: 68 percent / NaBH₄ / tetrahydrofuran; benzene; H₂O / 1 h / Ambient temperature

With pyridine; sodium tetrahydroborate; In tetrahydrofuran; dichloromethane; water; benzene;

DOI:10.1021/jm00175a003

Reference yield:

1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indole-3-acetyl chloride (20357-37-3) + 1,3-bis[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride (72155-37-4) → 1,2,3-tris[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride (72155-39-6)

Guidance literature:

With pyridine; In dichloromethane; for 96h; Ambient temperature;

DOI:10.1021/jm00175a003

upstream raw materials:

[1-(4-Chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]-acetic acid 3-{2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]-acetoxy}-2-oxo-propyl ester

1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indole-3-acetyl chloride

Downstream raw materials:

1,2,3-tris[1-(p-chlorobenzoyl)-5-methoxy-2-methylindole-3-acetyl]glyceride

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