C₁₇H₁₃NO₂

Base Information

• Chemical Name: C₁₇H₁₃NO₂
• CAS No.: 1040389-76-1
• Molecular Formula: C₁₇H₁₃NO₂
• Molecular Weight: 263.296
• Mol file: 1040389-76-1.mol

Synonyms:C₁₇H₁₃NO₂

Chemical Property of C₁₇H₁₃NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₇H₁₃NO₂

There total 1 articles about C₁₇H₁₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C26H33NO2Si (1040389-98-7) → C17H13NO2 (1040389-76-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1021/ol801257j

Reference yield: 77.0%

dimethyl diazomalonate (6773-29-1) + C17H13NO2 (1040389-76-1) → C22H19NO6 (1190202-46-0)

Guidance literature:

With dirhodium tetraacetate; In toluene; at 80 ℃; Inert atmosphere;

DOI:10.1021/ol901860b

Reference yield: 63.0%

2-Diazo-3-oxo-butyric acid methyl ester (24762-04-7) + C17H13NO2 (1040389-76-1) → C22H19NO5 (1190202-55-1)

Guidance literature:

With dirhodium tetraacetate; In toluene; at 80 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol901860b

upstream raw materials:

C₂₆H₃₃NO₂Si

Downstream raw materials:

C₃₁H₃₂N₂O₄

C₃₁H₃₂N₂O₄

C₂₂H₁₉NO₅

C₂₂H₁₉NO₆

Refernces

• 1、 Zhang, Xuejun,Hsung, Richard P.,Li, Hongyan,Zhang, Yu,Johnson, Whitney L.,Figueroa, Ruth. "A highly stereoselective synthesis of chiral α-amino-β-lactams via the Kinugasa reaction employing ynamides". supporting information; experimental part. p. 3477 - 3479. Retrieved 2009/05/27.