Technology Process of C16H23N3O5
There total 4 articles about C16H23N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di-tert-butyl dicarbonate;
In
dichloromethane;
Cooling with ice bath;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: isopropyl alcohol / Reflux
2: thionyl chloride / dichloromethane / 1 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 50 °C
4: hydrazine hydrate / ethanol / 2 h / 50 °C
5: di-tert-butyl dicarbonate / dichloromethane / Cooling with ice bath
With
thionyl chloride; di-tert-butyl dicarbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 50 °C
2: hydrazine hydrate / ethanol / 2 h / 50 °C
3: di-tert-butyl dicarbonate / dichloromethane / Cooling with ice bath
With
di-tert-butyl dicarbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;