3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

Base Information

Chemical Name:3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole
CAS No.:1298072-05-5
Molecular Formula:C₂₈H₂₈N₂O₅
Molecular Weight:472.541
Hs Code.:

Synonyms:3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

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Chemical Property of 3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

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Technology Process of 3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

There total 3 articles about 3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 22216-25-7
1-(3,5-dimethoxybenzyloxy)-3,5-dimethoxybenzene

: 21487-48-9
3-methyl-1-phenyl-1H-pyrazole-4-carbaldehyde

: 1298072-05-5
3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejoc.201001739

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 1298072-05-5
3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201001739

Reference yield:

: 877-88-3
3,5-dimethoxybenzyl bromide

: 1298072-05-5
3-methyl-1-phenyl-4-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201001739