C₁₂H₁₃FO₂

Base Information

Chemical Name:C₁₂H₁₃FO₂
CAS No.:1402585-80-1
Molecular Formula:C₁₂H₁₃FO₂
Molecular Weight:208.232
Hs Code.:

C<sub>12</sub>H<sub>13</sub>FO<sub>2</sub>

Synonyms:C₁₂H₁₃FO₂

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Chemical Property of C₁₂H₁₃FO₂

Chemical Property:

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Technology Process of C₁₂H₁₃FO₂

There total 3 articles about C₁₂H₁₃FO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1402585-79-8
(±)-methyl 2-(3-fluoro-4-iodophenyl)propanoate

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1402585-80-1
C₁₂H₁₃FO₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride; In N,N-dimethyl-formamide; at 23 ℃; for 15h; Inert atmosphere;

Reference yield:

: 90500-55-3
(±)-methyl 2-(4-amino-3-fluorophenyl)propanoate

: 1402585-80-1
C₁₂H₁₃FO₂

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 10 - 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / N,N-dimethyl-formamide / 15 h / 23 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; potassium iodide; lithium chloride; sodium nitrite; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 81937-33-9
2-(4-amino-3-fluorophenyl)propionic acid

: 1402585-80-1
C₁₂H₁₃FO₂

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / Cooling with ice

2: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 10 - 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / N,N-dimethyl-formamide / 15 h / 23 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; toluene-4-sulfonic acid; potassium iodide; lithium chloride; sodium nitrite; In water; N,N-dimethyl-formamide; acetonitrile;