N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

Base Information

Chemical Name:N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine
CAS No.:130340-77-1
Molecular Formula:C₂₄H₂₃N₃O₃
Molecular Weight:401.465
Hs Code.:

N<sup>1</sup>-(α-phenylpropionyl)-N<sup>1</sup>-(p-methylbenzyl)-N<sup>2</sup>-(p-nitrophenyl)formamidine

Synonyms:N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

Chemical Property:

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Technology Process of N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

There total 4 articles about N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2232-13-5
N¹,N²-di-(p-nitrophenyl)formamidine

: 130340-77-1
N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N / benzene / 1 h / Heating

2: 1.) LDA, 2.) HMPA / 1.) THF, hexane, 0 deg C, 2.) THF, 1 h, room temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; triethylamine; lithium diisopropyl amide; In benzene;
DOI:10.1248/cpb.38.1824

Reference yield:

: 130340-58-8
N,N-bis(p-nitrophenyliminomethyl)-p-nitroaniline

: 130340-77-1
N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 1 N NaOH / tetrahydrofuran / 1.5 h / Ambient temperature

2: 85 percent / Et₃N / benzene / 1 h / Heating

3: 1.) LDA, 2.) HMPA / 1.) THF, hexane, 0 deg C, 2.) THF, 1 h, room temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; benzene;
DOI:10.1248/cpb.38.1824

Reference yield:

: 128799-78-0
N¹-(p-chlorobenzoyl)-N¹,N²-di(p-nitrophenyl)formamidine

: 130340-77-1
N¹-(α-phenylpropionyl)-N¹-(p-methylbenzyl)-N²-(p-nitrophenyl)formamidine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi, diisopropylamine / 1.) THF, hexane, 0 deg C, 2.) 45 min, room temperature

2: 78 percent / 1 N NaOH / tetrahydrofuran / 1.5 h / Ambient temperature

3: 85 percent / Et₃N / benzene / 1 h / Heating

4: 1.) LDA, 2.) HMPA / 1.) THF, hexane, 0 deg C, 2.) THF, 1 h, room temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; n-butyllithium; triethylamine; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; benzene;
DOI:10.1248/cpb.38.1824