5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Base Information

Chemical Name:5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane
CAS No.:1429638-51-6
Molecular Formula:C₃₅H₅₀O₃Si₂
Molecular Weight:574.951
Hs Code.:

Synonyms:5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Suppliers and Price of 5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

There total 4 articles about 5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1429638-50-5
1-(benzyloxy)-2-((tert-butyldiphenylsilyloxy)methyl)-3-methylbut-3-en-2-ol

: C₁₅H₁₆ClFSi

: 1429638-51-6
5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Guidance literature:: at 100 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ol4005799

Reference yield:

: 172843-09-3
1-O-(tert-butyldiphenylsilyl)-1,3-dihydroxy-2-propanone

: 1429638-51-6
5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Guidance literature:: Multi-step reaction with 3 steps

1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 18 h / 0 - 20 °C / Inert atmosphere

2: tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

3: 72 h / 100 °C / Inert atmosphere

With trifluorormethanesulfonic acid; In tetrahydrofuran; dichloromethane; cyclohexane;
DOI:10.1021/ol4005799

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1429638-51-6
5-(benzyloxymethyl)-2,2,3,3,9,9-hexamethyl-8,8-diphenyl-5-(prop-1-en-2-yl)-4,7-dioxa-3,8-disiladecane

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 18 h / 0 - 20 °C / Inert atmosphere

3: tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

4: 72 h / 100 °C / Inert atmosphere

With 1H-imidazole; trifluorormethanesulfonic acid; In tetrahydrofuran; dichloromethane; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/ol4005799