3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol

Base Information

• Chemical Name: 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol
• CAS No.: 81253-74-9
• Molecular Formula: C₂₁H₂₇N₃O₆
• Molecular Weight: 417.462

Synonyms:3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol

Chemical Property of 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol

Chemical Property:

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Technology Process of 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol

There total 3 articles about 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-{2-[3-(2,3-Dihydro-benzo[1,4]dioxin-5-yloxy)-2-hydroxy-propylamino]-ethyl}-2-(4-nitro-phenoxy)-acetamide (58827-92-2) → 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol (81253-74-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;

DOI:10.1021/jm00354a005

Reference yield:

ethyl 4-nitrophenoxyacetate (19076-89-2) → 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol (81253-74-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 27 percent / 18 h / 100 °C

2: H₂ / 30percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1021/jm00354a005

Reference yield:

1-(2-Amino-ethylamino)-3-(2,3-dihydro-benzo[1,4]dioxin-5-yloxy)-propan-2-ol (58827-91-1) → 3-<<2-<(4-aminophenoxy)acetamido>ethyl>amino>-1-<(1,4-benzodioxan-5-yl)oxy>propan-2-ol (81253-74-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 27 percent / 18 h / 100 °C

2: H₂ / 30percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1021/jm00354a005

upstream raw materials:

N-{2-[3-(2,3-Dihydro-benzo[1,4]dioxin-5-yloxy)-2-hydroxy-propylamino]-ethyl}-2-(4-nitro-phenoxy)-acetamide

ethyl 4-nitrophenoxyacetate

1-(2-Amino-ethylamino)-3-(2,3-dihydro-benzo[1,4]dioxin-5-yloxy)-propan-2-ol

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