butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

Base Information

Chemical Name:butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate
CAS No.:1314773-72-2
Molecular Formula:C₂₃H₂₇N₃O₅S
Molecular Weight:457.55
Hs Code.:

Synonyms:butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

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Chemical Property of butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

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Technology Process of butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

There total 4 articles about butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.2%

: 1314774-40-7
butyl 6-(2-methoxy-4-phenyl-4,5-dihydroimidazol-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

: 1314773-72-2
butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

Guidance literature:: With hydrogenchloride; methanol; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2011.04.042

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1314773-72-2
butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide / dichloromethane

2: hydrogenchloride

3: sodium hydrogencarbonate / water; acetone / 2 h / 20 °C

4: hydrogenchloride; methanol / diethyl ether / 3 h / 20 °C

With hydrogenchloride; methanol; N-Bromosuccinimide; sodium hydrogencarbonate; In diethyl ether; dichloromethane; water; acetone;
DOI:10.1016/j.ejmech.2011.04.042

Reference yield:

: 185098-76-4
2-bromo-1-phenylethyl cyanamide

: 1314773-72-2
butyl 6-(2-oxo-4-phenylimidazolidin-1-ylsulfonyl)-3,4-dihydroquinoline-1(2H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride

2: sodium hydrogencarbonate / water; acetone / 2 h / 20 °C

3: hydrogenchloride; methanol / diethyl ether / 3 h / 20 °C

With hydrogenchloride; methanol; sodium hydrogencarbonate; In diethyl ether; water; acetone;
DOI:10.1016/j.ejmech.2011.04.042