C₃₀H₂₂O₄

Base Information

Chemical Name:C₃₀H₂₂O₄
CAS No.:1266348-24-6
Molecular Formula:C₃₀H₂₂O₄
Molecular Weight:446.502
Hs Code.:

C<sub>30</sub>H<sub>22</sub>O<sub>4</sub>

Synonyms:C₃₀H₂₂O₄

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Chemical Property of C₃₀H₂₂O₄

Chemical Property:

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Technology Process of C₃₀H₂₂O₄

There total 6 articles about C₃₀H₂₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 66-98-8
4,4'-diformylbiphenyl

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 1266348-24-6
C₃₀H₂₂O₄

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 48h;
DOI:10.1007/s12272-010-1205-2

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1266348-24-6
C₃₀H₂₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 4 h / Reflux

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

3: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 20 - 100 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux; Cooling with ice

5: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux

6: potassium hydroxide / methanol / 48 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; lithium aluminium tetrahydride; sulfuric acid; potassium acetate; pyridinium chlorochromate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 3: Suzuki-Miyaura reaction / 6: Claisen-Schmidt condensation;
DOI:10.1007/s12272-010-1205-2

Reference yield:

: 5798-75-4
Ethyl 4-bromobenzoate

: 1266348-24-6
C₃₀H₂₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

2: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 20 - 100 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux; Cooling with ice

4: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux

5: potassium hydroxide / methanol / 48 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; lithium aluminium tetrahydride; potassium acetate; pyridinium chlorochromate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 2: Suzuki-Miyaura reaction / 5: Claisen-Schmidt condensation;
DOI:10.1007/s12272-010-1205-2