(4As,8as)-1-methyldecahydroquinoxaline

Base Information

Chemical Name:(4As,8as)-1-methyldecahydroquinoxaline
CAS No.:6335-62-2
Molecular Formula:C₉H₁₈N₂
Molecular Weight:154.255
Hs Code.:
NSC Number:28005
DSSTox Substance ID:DTXSID00979489
Mol file:6335-62-2.mol

Synonyms:(4as,8as)-1-methyldecahydroquinoxaline;6335-62-2;(4aS,8aS)-4-methyl-2,3,4a,5,6,7,8,8a-octahydro-1H-quinoxaline;NSC28005;1-methyldecahydroquinoxaline;SCHEMBL15918980;DTXSID00979489;QUINOXALINE, DECAHYDRO-1-METHYL-, TRANS- (8CI,9CI);NSC-28005

Suppliers and Price of (4As,8as)-1-methyldecahydroquinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (4As,8as)-1-methyldecahydroquinoxaline

Chemical Property:

Vapor Pressure:0.118mmHg at 25°C
Boiling Point:219.7°C at 760 mmHg
Flash Point:84.4°C
PSA：15.27000
Density:0.931g/cm³
LogP:1.09930
XLogP3:0.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:154.146998583
Heavy Atom Count:11
Complexity:136

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCNC2C1CCCC2
Isomeric SMILES:CN1CCN[C@@H]2[C@@H]1CCCC2

Technology Process of (4As,8as)-1-methyldecahydroquinoxaline

There total 2 articles about (4As,8as)-1-methyldecahydroquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 114563-19-8
trans-3-Methyl-decahydro-2(1H)-quinoxalinone

: 5467-39-0,6335-62-2
trans-1-Methyldecahydroquinoxaline

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 1h;
DOI:10.1002/jhet.5570240512

Reference yield:

: 51066-08-1
7-methyl-7-azabicyclo[4.1.0]heptane

: 5467-39-0,6335-62-2
trans-1-Methyldecahydroquinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NH₄Cl / H₂O / 2 h / Heating

2: 44 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

With lithium aluminium tetrahydride; ammonium chloride; In diethyl ether; water;
DOI:10.1002/jhet.5570240512