C₄₅H₇₈O₉Si₂

Base Information

Chemical Name:C₄₅H₇₈O₉Si₂
CAS No.:177320-40-0
Molecular Formula:C₄₅H₇₈O₉Si₂
Molecular Weight:819.28
Hs Code.:

C<sub>45</sub>H<sub>78</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₄₅H₇₈O₉Si₂

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Chemical Property of C₄₅H₇₈O₉Si₂

Chemical Property:

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Technology Process of C₄₅H₇₈O₉Si₂

There total 26 articles about C₄₅H₇₈O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108814-35-3
(2R,3R,4S)-1-(benzyloxy)-2,4-dimethyl-3-hydroxy-5-hexene

: 177320-40-0
C₄₅H₇₈O₉Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: Et₃N, DMAP / CH₂Cl₂

2: 1.) 9-BBN, 2.) H₂O₂, aq. NaOH / 1.) THF

3: 1.) Pr₄NRuO₄, NMO, 4 Angstroem molecular sieves, 2.) NaClO₂, NaH₂PO₄, 2-methylbut-2-ene / 1.) CH₂Cl₂, 2.) aq. t-BuOH

4: aq. HF / acetonitrile

5: HCO₂NH₄ / 5percent Pd/C / methanol

6: imidazole / dimethylformamide

7: LDA / tetrahydrofuran / -78 °C

8: 82 percent / BuLi / tetrahydrofuran

9: Bu₃SnH, AIBN / 100 °C

With 1H-imidazole; dmap; sodium hydroxide; sodium chlorite; sodium dihydrogenphosphate; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; hydrogen fluoride; dihydrogen peroxide; tri-n-butyl-tin hydride; ammonium formate; triethylamine; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/CC9960000871

Reference yield:

: 177320-38-6
(4S,5S)-5-((R)-2-Benzyloxy-1-methyl-ethyl)-4-methyl-dihydro-furan-2-one

: 177320-40-0
C₄₅H₇₈O₉Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: HCO₂NH₄ / 5percent Pd/C / methanol

2: imidazole / dimethylformamide

3: LDA / tetrahydrofuran / -78 °C

4: 82 percent / BuLi / tetrahydrofuran

5: Bu₃SnH, AIBN / 100 °C

With 1H-imidazole; n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; ammonium formate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/CC9960000871

Reference yield:

: [(1S,2S)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-triethyl-silane

: 177320-40-0
C₄₅H₇₈O₉Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) 9-BBN, 2.) H₂O₂, aq. NaOH / 1.) THF

2: 1.) Pr₄NRuO₄, NMO, 4 Angstroem molecular sieves, 2.) NaClO₂, NaH₂PO₄, 2-methylbut-2-ene / 1.) CH₂Cl₂, 2.) aq. t-BuOH

3: aq. HF / acetonitrile

4: HCO₂NH₄ / 5percent Pd/C / methanol

5: imidazole / dimethylformamide

6: LDA / tetrahydrofuran / -78 °C

7: 82 percent / BuLi / tetrahydrofuran

8: Bu₃SnH, AIBN / 100 °C

With 1H-imidazole; sodium hydroxide; sodium chlorite; sodium dihydrogenphosphate; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; hydrogen fluoride; dihydrogen peroxide; tri-n-butyl-tin hydride; ammonium formate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/CC9960000871