Technology Process of C17H24O4
There total 8 articles about C17H24O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; lithium hydroxide;
In
tetrahydrofuran; water;
at 0 ℃;
for 1.5h;
chemoselective reaction;
DOI:10.1039/c0cc05215a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene / 4.08 h / 180 °C / Inert atmosphere
2.1: C32H12BF24(1-)*C39H50IrNOP(1+); hydrogen / dichloromethane / 18 h / 20 °C / Autoclave
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.5 h / 0 °C
With
C32H12BF24(1-)*C39H50IrNOP(1+); hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
1.1: oxy-Cope rearrangement;
DOI:10.1039/c0cc05215a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.5 h / 0 °C
With
dihydrogen peroxide; sodium hexamethyldisilazane; lithium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1039/c0cc05215a
