N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine

Base Information

• Chemical Name: N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine
• CAS No.: 1445383-58-3
• Molecular Formula: C₁₂H₁₀ClFN₅OPS
• Molecular Weight: 357.735

Synonyms:N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine

Chemical Property of N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine

Chemical Property:

Purity/Quality:

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Technology Process of N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine

There total 1 articles about N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

[(2-thioxo-2,3-dihydro-2λ5-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)amino]methanenitrile (1445383-00-5) + 2-chloro-4-fluoroaniline (2106-02-7) → N-(2-chloro-4-fluorophenyl)-N'-(2-thioxo-2,3-dihydro-2λ5-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)guanidine (1445383-58-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 50 - 60 ℃; for 2h;

DOI:10.1248/cpb.c12-00582

upstream raw materials:

[(2-thioxo-2,3-dihydro-2λ⁵-pyrido[2,3-d][1,3,2]oxazaphosphol-2-yl)amino]methanenitrile

2-chloro-4-fluoroaniline

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