C₄₀H₅₇NO₅S

Base Information

Chemical Name:C₄₀H₅₇NO₅S
CAS No.:1354656-85-1
Molecular Formula:C₄₀H₅₇NO₅S
Molecular Weight:663.962
Hs Code.:

C<sub>40</sub>H<sub>57</sub>NO<sub>5</sub>S

Synonyms:C₄₀H₅₇NO₅S

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Chemical Property of C₄₀H₅₇NO₅S

Chemical Property:

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Technology Process of C₄₀H₅₇NO₅S

There total 9 articles about C₄₀H₅₇NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 174627-66-8
(2S,4S,6S)-2,4,6-trimethyl-1-nonanal

: 187324-66-9
(1R,2S)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate

: 1354656-85-1
C₄₀H₅₇NO₅S

Guidance literature:: (1R,2S)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate; With triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In dichloromethane; at -78 ℃; for 5h; Inert atmosphere;

(2S,4S,6S)-2,4,6-trimethyl-1-nonanal; In dichloromethane; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo202330b

Reference yield:

: C₂₆H₂₇NO₅

: 1354656-85-1
C₄₀H₅₇NO₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: C₃₂H₁₂BF₂₄^(1-)*C₃₉H₅₀IrNOP⁽¹⁺⁾; hydrogen / dichloromethane / 18 h / 20 °C / 60006 - 67506.8 Torr / Inert atmosphere; Autoclave

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 0 °C / Inert atmosphere

4.1: 1H-imidazole; dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: methanol; potassium carbonate / 18 h / 20 °C / Inert atmosphere

6.1: pyridine; dmap / dichloromethane / 18 h / 40 °C / Inert atmosphere

7.1: magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

7.2: -20 - 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / Inert atmosphere

9.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran; dimethyl sulfoxide / 5 h / 20 °C / Inert atmosphere

10.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / dichloromethane / 5 h / -78 °C / Inert atmosphere

10.2: 3 h / -78 °C / Inert atmosphere

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; C₃₂H₁₂BF₂₄^(1-)*C₃₉H₅₀IrNOP⁽¹⁺⁾; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; potassium carbonate; magnesium; triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/jo202330b

Reference yield:

: 1283732-98-8
C₂₆H₂₇NO₅

: 1354656-85-1
C₄₀H₅₇NO₅S

Guidance literature:: Multi-step reaction with 11 steps

1.1: toluene / 4 h / 180 °C / Inert atmosphere

2.1: C₃₂H₁₂BF₂₄^(1-)*C₃₉H₅₀IrNOP⁽¹⁺⁾; hydrogen / dichloromethane / 18 h / 20 °C / 60006 - 67506.8 Torr / Inert atmosphere; Autoclave

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

4.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 0 °C / Inert atmosphere

5.1: 1H-imidazole; dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.1: methanol; potassium carbonate / 18 h / 20 °C / Inert atmosphere

7.1: pyridine; dmap / dichloromethane / 18 h / 40 °C / Inert atmosphere

8.1: magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

8.2: -20 - 20 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / Inert atmosphere

10.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran; dimethyl sulfoxide / 5 h / 20 °C / Inert atmosphere

11.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / dichloromethane / 5 h / -78 °C / Inert atmosphere

11.2: 3 h / -78 °C / Inert atmosphere

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; C₃₂H₁₂BF₂₄^(1-)*C₃₉H₅₀IrNOP⁽¹⁺⁾; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; potassium carbonate; magnesium; triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; toluene; 1.1: Cope rearrangement;
DOI:10.1021/jo202330b