Technology Process of C71H116N2O8
There total 5 articles about C71H116N2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
tetrahydrofuran;
for 12h;
Reflux;
DOI:10.1021/cm300762j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3 h / 0 °C / Inert atmosphere
2: hydrazine hydrate / tetrahydrofuran; ethanol / 1 h / Reflux
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 25 °C
4: sodium hydroxide / tetrahydrofuran / 12 h / Reflux
With
di-isopropyl azodicarboxylate; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/cm300762j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine hydrate / tetrahydrofuran; ethanol / 1 h / Reflux
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 25 °C
3: sodium hydroxide / tetrahydrofuran / 12 h / Reflux
With
benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/cm300762j
