5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

Base Information

Chemical Name:5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide
CAS No.:1416698-98-0
Molecular Formula:C₂₃H₁₉Cl₃N₄O₅S
Molecular Weight:569.853
Hs Code.:

Synonyms:5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

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Chemical Property of 5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

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Technology Process of 5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

There total 11 articles about 5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114129-35-0
methyl 4-(methylsulfinyl)benzoate

: 1416698-98-0
5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

Guidance literature:: Multi-step reaction with 7 steps

1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

2: pyridine / dichloromethane; toluene / 3 h / 15 - 30 °C / Inert atmosphere

3: water; sodium hydroxide / tetrahydrofuran / 3 h / 25 - 30 °C

4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

5: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

6: sulfuric acid / 0 - 5 °C

7: triethylamine / tetrahydrofuran / 2 h / 0 - 30 °C

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform; toluene;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

: 4920-80-3
3-methoxy-2-nitrobenzoic acid

: 1416698-98-0
5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine; trichlorophosphate / acetonitrile / 1 h / 0 - 30 °C / Inert atmosphere

2: tin(II) chloride dihdyrate / ethyl acetate / 2 h / 25 - 30 °C

3: N-chloro-succinimide / benzene / 24 h / 25 - 65 °C

4: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

5: sulfuric acid / 0 - 5 °C

6: triethylamine / tetrahydrofuran / 2 h / 0 - 30 °C

With pyridine; N-chloro-succinimide; tin(II) chloride dihdyrate; sulfuric acid; triethylamine; trichlorophosphate; In tetrahydrofuran; ethyl acetate; acetonitrile; benzene;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

: 1147096-51-2
methyl 4-[imino(methyl)oxo-λ⁶-sulfanyl]benzoate

: 1416698-98-0
5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)-3-methoxybenzamide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / dichloromethane; toluene / 3 h / 15 - 30 °C / Inert atmosphere

2: water; sodium hydroxide / tetrahydrofuran / 3 h / 25 - 30 °C

3: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

4: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

5: sulfuric acid / 0 - 5 °C

6: triethylamine / tetrahydrofuran / 2 h / 0 - 30 °C

With pyridine; oxalyl dichloride; sulfuric acid; water; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.ejmech.2012.10.005