1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

Base Information

Chemical Name:1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone
CAS No.:1414628-82-2
Molecular Formula:C₂₇H₃₁N₃O₄
Molecular Weight:461.561
Hs Code.:

Synonyms:1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

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Chemical Property of 1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

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Technology Process of 1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

There total 1 articles about 1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31252-42-3
4-benzylpyperidine

: C₁₅H₁₅ClN₂O₄

: 1414628-82-2
1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

Guidance literature:: C₁₅H₁₅ClN₂O₄; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

4-benzylpyperidine; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/jm301508d

Reference yield: 70.0%

: 1414628-82-2
1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

: 1414628-89-9
C₂₂H₂₃N₃O₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/jm301508d

Reference yield:

: 1414628-82-2
1-[(tert-butyl-1H-indol-5-yl-carbamate)4-benzilpiperdin-1-yl]-2-oxoethanone

: 1414628-97-9
C₂₃H₂₅N₃O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

2: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm301508d