7-hexadecynyl tosylate

Base Information

• Chemical Name: 7-hexadecynyl tosylate
• CAS No.: 1246077-93-9
• Molecular Formula: C₂₃H₃₆O₃S
• Molecular Weight: 392.603
• Mol file: 1246077-93-9.mol

Synonyms:7-hexadecynyl tosylate

Chemical Property of 7-hexadecynyl tosylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-hexadecynyl tosylate

There total 1 articles about 7-hexadecynyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

hexadec-7-yn-1-ol (822-21-9) + p-toluenesulfonyl chloride (98-59-9) → 7-hexadecynyl tosylate (1246077-93-9)

Guidance literature:

With pyridine; at 5 - 10 ℃;

DOI:10.1016/j.tet.2010.06.080

Reference yield: 72.0%

7-hexadecynyl tosylate (1246077-93-9) → 7-hexadecynyl iodide (29747-19-1)

Guidance literature:

With sodium iodide; In N,N-dimethyl-formamide; at 20 - 80 ℃;

DOI:10.1016/j.tet.2010.06.080

upstream raw materials:

hexadec-7-yn-1-ol

p-toluenesulfonyl chloride

Downstream raw materials:

7-hexadecynyl iodide