methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside
CAS No.:122992-49-8
Molecular Formula:C₄₃H₅₁NO₁₆
Molecular Weight:837.875
Hs Code.:

Synonyms:methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

There total 4 articles about methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 110236-56-1
methyl N-benzyloxycarbonyl-2-deoxy-3,6-di-O-benzylglucopyranoside

: 439-03-2,439-04-3,439-05-4,2823-44-1,2823-46-3,3934-29-0,4163-44-4,4163-45-5,20409-31-8,23235-96-3,51897-75-7,51897-76-8,51897-77-9,57573-38-3,62561-28-8,126641-47-2
2,3,4,6-tetra-O-acetyl-1-fluoro-α-D-glucopyranose

: 122992-49-8
methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; (polyethylene vessel) 1.) -20 deg C, 2 h, 2.) 0 deg C, overnight;

Reference yield: 25.0%

: 74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,127061-80-7,142831-80-9
2,3,4,6-tetra-O-acetyl-d-glucopyranosyl trichloroacetimidate

: 110236-56-1
methyl N-benzyloxycarbonyl-2-deoxy-3,6-di-O-benzylglucopyranoside

: 122992-49-8
methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; polyethylene vessel!;

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 122992-49-8
methyl 3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 2-aminoethanol

3: 25 percent / boron trifluoride etherate / CH₂Cl₂ / polyethylene vessel!

With boron trifluoride diethyl etherate; ethanolamine; In dichloromethane;