3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

Base Information

Chemical Name:3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol
CAS No.:883196-70-1
Molecular Formula:C₇₅H₁₂₈O₇
Molecular Weight:1141.84
Hs Code.:

Synonyms:3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

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Chemical Property of 3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

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Technology Process of 3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

There total 12 articles about 3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 883196-69-8
methyl 3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propionate

: 883196-70-1
3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ja060062a

Reference yield:

: 2150-43-8
3,4-dihydroxybenzoic acid methyl ester

: 883196-70-1
3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

Guidance literature:: Multi-step reaction with 8 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 8 h / 75 °C

2: 94 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

3: pyridinium chlorochromate / CH₂Cl₂ / 20 °C

4: 90 percent / morpholine; AcOH / Heating

5: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating

6: 91 percent / H₂ / Pd/C / ethanol

7: 80 percent / K₂CO₃ / dimethylformamide / 20 h / 80 °C

8: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

With morpholine; lithium aluminium tetrahydride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 4: Knoevenagel condensation;
DOI:10.1021/ja060062a

Reference yield:

: 54429-62-8
(E)-3-(3,4-bis(benzyloxy)phenyl)acrylic acid

: 883196-70-1
3-{3,4-bis[3-(3,4-bis(dodecyl-1-oxy)phenyl)propyl-1-oxy]phenyl}propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating

2: 91 percent / H₂ / Pd/C / ethanol

3: 80 percent / K₂CO₃ / dimethylformamide / 20 h / 80 °C

4: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

With lithium aluminium tetrahydride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja060062a