N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

Base Information

Chemical Name:N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide
CAS No.:1574609-55-4
Molecular Formula:C₂₇H₄₈N₂O₃Sn
Molecular Weight:567.4
Hs Code.:

Synonyms:N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

Suppliers and Price of N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

There total 2 articles about N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.4%

: 813-19-4
bis(tri-n-butyltin)

: 84226-06-2,130383-75-4
[123I]-IBZM

: 1574609-55-4
N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 100 ℃; Sealed tube; Inert atmosphere;

Reference yield:

: FLA 981

: 1574609-55-4
N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-hydroxy-6-methoxy-3-tri-butylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: Iodine monochloride / methanol; dichloromethane / 2 h / 50 °C

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 100 °C / Sealed tube; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Iodine monochloride; triethylamine; In methanol; dichloromethane;