14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate

Base Information

• Chemical Name: 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate
• CAS No.: 63689-45-2
• Molecular Formula: C₂₃H₃₂NO₂*C₂₄H₂₀B
• Molecular Weight: 673.746

Synonyms:14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate

Chemical Property of 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate

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Technology Process of 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate

There total 3 articles about 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5,6,7,8-hexahydro-2H-benzo[6,7]cyclohepta[1,2-b]oxepine (63689-22-5) → 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate (63689-45-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) AgBF₄, ClCH₂CH₂Cl, (ii) /BRN= 4652394/, H₂O

2: (i) AgBF₄, ClCH₂CH₂Cl, (ii) /BRN= 3599783/, H₂O

DOI:10.1021/jo00862a009

Reference yield:

N-(2-Chlorethyliden)cyclohexylamin-oxid (37898-41-2) → 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate (63689-45-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) AgBF₄, ClCH₂CH₂Cl, (ii) /BRN= 4652394/, H₂O

2: (i) AgBF₄, ClCH₂CH₂Cl, (ii) /BRN= 3599783/, H₂O

DOI:10.1021/jo00862a009

Reference yield:

sodium tetraphenyl borate (143-66-8) + 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabutano-benzo[6,7]cyclohepta[1,2-b]oxepine-15-carbonitrile (63689-25-8) → 14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-2-eno-benzo[6,7]cyclohepta[1,2-b]oxepinium; tetraphenylborate (63689-45-2)

Guidance literature:

Multistep reaction; (i) AgBF₄, ClCH₂CH₂Cl, (ii) /BRN= 3599783/, H₂O;

DOI:10.1021/jo00862a009

upstream raw materials:

sodium tetraphenyl borate

14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabutano-benzo[6,7]cyclohepta[1,2-b]oxepine-15-carbonitrile

3,4,5,6,7,8-hexahydro-2H-benzo[6,7]cyclohepta[1,2-b]oxepine

N-(2-Chlorethyliden)cyclohexylamin-oxid

Downstream raw materials:

14-cyclohexyl-2,3,4,5,7,8-hexahydro-6H-12b,5a-[1]oxa[2]azabut-3-eno-benzo[6,7]cyclohepta[1,2-b]oxepine

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