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2-iodo-3'-phenoxybiphenyl

Base Information
  • Chemical Name:2-iodo-3'-phenoxybiphenyl
  • CAS No.:607731-69-1
  • Molecular Formula:C18H13IO
  • Molecular Weight:372.205
  • Hs Code.:
2-iodo-3'-phenoxybiphenyl

Synonyms:2-iodo-3'-phenoxybiphenyl

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Chemical Property of 2-iodo-3'-phenoxybiphenyl
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Technology Process of 2-iodo-3'-phenoxybiphenyl

There total 5 articles about 2-iodo-3'-phenoxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With copper diacetate; oxygen; triethylamine; In dichloromethane; at 20 ℃; for 48h; under 760 Torr;
DOI:10.1021/ja035121o
Guidance literature:
Multi-step reaction with 3 steps
1.1: Mg / tetrahydrofuran
1.2: tetrahydrofuran / 14 h / 20 °C
1.3: 40 percent / iodine / tetrahydrofuran / 0.5 h / 20 °C
2.1: 98 percent / BBr3 / CH2Cl2 / -78 - 20 °C
3.1: 46 percent / Cu(OAc)2; triethylamine; oxygen / CH2Cl2 / 48 h / 20 °C / 760 Torr
With copper diacetate; oxygen; boron tribromide; magnesium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo048788h
Guidance literature:
Multi-step reaction with 2 steps
1: 98 percent / BBr3 / CH2Cl2 / -78 - 20 °C
2: 46 percent / Cu(OAc)2; triethylamine; oxygen / CH2Cl2 / 48 h / 20 °C / 760 Torr
With copper diacetate; oxygen; boron tribromide; triethylamine; In dichloromethane;
DOI:10.1021/jo048788h
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