2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Base Information

• Chemical Name: 2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol
• CAS No.: 501912-09-0
• Molecular Formula: C₁₉H₃₂N₂O₄
• Molecular Weight: 352.474

Synonyms:2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Chemical Property of 2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Chemical Property:

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Technology Process of 2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

There total 2 articles about 2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine (14384-45-3) + 5-tert-butyl-3,4-dimethoxybenzaldehyde (333401-63-1) → 2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol (501912-09-0)

Guidance literature:

In methanol; for 12h; Heating;

DOI:10.1021/ja020715x

Reference yield:

4-bromo-6-tert-butylcatechol dimethyl ether (168985-94-2) → 2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol (501912-09-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: t-BuLi / pentane; tetrahydrofuran / 1 h / -78 °C

1.2: 94 percent / pentane; tetrahydrofuran / 12 h / 20 °C

2.1: 91 percent / methanol / 12 h / Heating

With tert.-butyl lithium; In tetrahydrofuran; methanol; pentane;

DOI:10.1021/ja020715x

Reference yield: 90.0%

2-(3-tert-butyl-4,5-dimethoxy-phenyl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol (501912-09-0) → C19H29N2O4

Guidance literature:

With sodium periodate; In chloroform; water; for 0.166667h;

DOI:10.1021/ja020715x

upstream raw materials:

N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

5-tert-butyl-3,4-dimethoxybenzaldehyde

4-bromo-6-tert-butylcatechol dimethyl ether

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