N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide

Base Information

Chemical Name:N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide
CAS No.:1108745-20-5
Molecular Formula:C₄₅H₃₆F₂N₆O₄
Molecular Weight:762.815
Hs Code.:

Synonyms:N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide

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Chemical Property of N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide

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Technology Process of N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide

There total 1 articles about N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 942271-64-9
4-(4-methyl-piperazin-1-yl)-2-nitro-benzoic acid hydrochloride

: 1108745-18-1
(3-amino-1-trityl-1H-indazol-5-yl)-(3,5-difluoro-phenyl)-methanone

: 1108745-20-5
N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide

Guidance literature:: 4-(4-methyl-piperazin-1-yl)-2-nitro-benzoic acid hydrochloride; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 20 ℃;

(3-amino-1-trityl-1H-indazol-5-yl)-(3,5-difluoro-phenyl)-methanone; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 - 75 ℃; for 2h;

Reference yield: 78.0%

: 1108745-20-5
N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide

: 1108745-22-7
N-[5-(3,5-difluoro-benzoyl)-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitro-benzamide

Guidance literature:: N-[5-(3,5-difluoro-benzoyl)-1-trityl-1H-indazol-3-yl]-4-(4-methyl-piperazin-1-yl)-2-nitrobenzamide; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With water; sodium hydrogencarbonate; In dichloromethane;