trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide

Base Information

• Chemical Name: trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide
• CAS No.: 1245720-27-7
• Molecular Formula: C₁₉H₁₇F₃NO₃PS
• Molecular Weight: 427.384
• Mol file: 1245720-27-7.mol

Synonyms:trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide

Chemical Property of trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide

There total 3 articles about trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichlorotriphenylphosphorane (2526-64-9) → trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide (1245720-27-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrachloromethane / 2 h / 20 °C

2: water / chloroform-d1

With water; In tetrachloromethane; chloroform-d1;

DOI:10.1134/S107036321006023X

Reference yield:

triphenylphosphine (603-35-0) → trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide (1245720-27-7)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 16 h / 20 °C / Inert atmosphere

2: water / chloroform-d1

With water; In chloroform-d1; benzene;

DOI:10.1134/S107036321006023X

Reference yield:

trifluoro-N-(triphenyl-λ5-phosphanylidene)methanesulfonamide → trifluoro-N-[hydroxy(triphenyl)phosphoranyl]methanesulfonamide (1245720-27-7)

Guidance literature:

With water; In chloroform-d1;

DOI:10.1134/S107036321006023X

upstream raw materials:

triphenylphosphine

dichlorotriphenylphosphorane

Downstream raw materials:

Trifluoromethanesulfonamide

Triphenylphosphine oxide