[(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)][CH₃B(C₆F₅)3]

Base Information

• Chemical Name: [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)][CH₃B(C₆F₅)3]
• CAS No.: 166987-10-6
• Molecular Formula: C₁₇H₂₃OZr*C₁₉H₃BF₁₅
• Molecular Weight: 861.613

Synonyms:[(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)][CH₃B(C₆F₅)3]

Chemical Property of [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)][CH₃B(C₆F₅)3]

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Technology Process of [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)][CH₃B(C₆F₅)3]

There total 1 articles about [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)][CH₃B(C₆F₅)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)(CH3) (166544-85-0) + tris(pentafluorophenyl)borate (1109-15-5) → [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)](1+)*[CH3B(C6F5)3](1-) = [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)][CH3B(C6F5)3] (166987-10-6)

Guidance literature:

In dichloromethane; under N2; a soln. of B(C6F5)3 in CH2Cl2 was added to a soln. of the Zr complex in CH2Cl2, the mixt. was stirred at 23°C for 10 min; the solvent was removed under vac., the residue was crystd. from CH2Cl2/pentane; elem. anal.;

DOI:10.1021/ja000989p

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)](1+)*[CH3B(C6F5)3](1-) = [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)][CH3B(C6F5)3] (166987-10-6) → [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)(C4H8O)](1+)*[CH3B(C6F5)3](1-) = [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)(C4H8O)][CH3B(C6F5)3] (166987-11-7)

Guidance literature:

In dichloromethane-d2; under N2; THF was added to a soln. of the Zr complex in CD2Cl2, the mixt. was vigorously agitated; the volatiles were removed under vac., CD2Cl2 was added, monitored by NMR;

DOI:10.1021/ja000989p

Reference yield:

diethyl ether (60-29-7,927820-24-4) + [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)](1+)*[CH3B(C6F5)3](1-) = [(C5H5)2Zr(OC(CH3)2(CH2)2CHCH2)][CH3B(C6F5)3] (166987-10-6) → [(C5H5)2Zr(OC(CH3)2CH2CH2CHCH2)(CH3CH2)2O](1+)*[CH3B(C6F5)3](1-)=[(C5H5)2Zr(OC(CH3)2CH2CH2CHCH2)(CH3CH2)2O][CH3B(C6F5)3] (166987-12-8)

Guidance literature:

In dichloromethane-d2; under N2; (CH3CH2)2O was added to a soln. of the Zr complex in CD2Cl2, the mixt. was vigorously agitated; the volatiles were removed under vac., CD2Cl2 was added, monitored by NMR;

DOI:10.1021/ja000989p

upstream raw materials:

(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)(CH₃)

tris(pentafluorophenyl)borate

Downstream raw materials:

[(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)(C₄H₈O)]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) = [(C₅H₅)2Zr(OC(CH₃)2(CH₂)2CHCH₂)(C₄H₈O)][CH₃B(C₆F₅)3]

[(C₅H₅)2Zr(OC(CH₃)2CH₂CH₂CHCH₂)(CH₃CH₂)2O]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)=[(C₅H₅)2Zr(OC(CH₃)2CH₂CH₂CHCH₂)(CH₃CH₂)2O][CH₃B(C₆F₅)3]

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