Technology Process of (S)-N-(1-cyanoethyl)-4-octylbenzmide
There total 4 articles about (S)-N-(1-cyanoethyl)-4-octylbenzmide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol
2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 15h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 15 h / 20 °C
1.3: Reflux; Inert atmosphere
2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol
3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
