8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

Base Information

Chemical Name:8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline
CAS No.:444564-97-0
Molecular Formula:C₂₁H₂₁IN₂O₃
Molecular Weight:476.314
Hs Code.:

Synonyms:8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

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Chemical Property of 8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

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Technology Process of 8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

There total 1 articles about 8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 444564-96-9
8-benzyloxy-6-(tert-butyloxycarbonylamino)quinoline

: 444564-97-0
8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

Guidance literature:: With N-iodo-succinimide; In acetonitrile; for 1h; regiospecific reaction; Reflux;
DOI:10.1021/jm9008746

Reference yield: 93.0%

: 444564-97-0
8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

: 106-95-6
allyl bromide

: 8-benzyloxy-6-[N-(tert-butyloxycarbonyl)-N-(2-propenyl)amino]-5-iodoquinoline

Guidance literature:: 8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline; With sodium hydride; In N,N-dimethyl-formamide; for 0.583333h;

allyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 3.25h;
DOI:10.1021/jm9008746

Reference yield: 83.0%

: 36255-44-4
3-bromopropanal dimethyl acetal

: 444564-97-0
8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline

: 444564-98-1
8-benzyloxy-6-[N-(tert-butyloxycarbonyl)-N-(3,3-dimethoxypropyl)amino]-5-iodoquinoline

Guidance literature:: 8-benzyloxy-6-(tert-butyloxycarbonylamino)-5-iodoquinoline; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

3-bromopropanal dimethyl acetal; In N,N-dimethyl-formamide; at 20 ℃; for 22h; Inert atmosphere;
DOI:10.1021/jm9008746