(4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate

Base Information

Chemical Name:(4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate
CAS No.:1448228-32-7
Molecular Formula:C₃₃H₂₉NO₅S
Molecular Weight:551.663
Hs Code.:

Synonyms:(4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate

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Technology Process of (4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate

There total 2 articles about (4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1448228-13-4
4-(4-methyl-N-tosylbenzamido)-4-phenylbut-2-yn-1-yl 4-methylbenzoate

: 1448228-32-7
(4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate

Guidance literature:: With silver tetrafluoroborate; In toluene; at 80 ℃; for 10h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/jo401330t

Reference yield:

: C₁₇H₁₇NO₃S

: 1448228-32-7
(4-(phenyl(tosyl)methyl)-2-(p-tolyl)oxazol-5-yl)methyl 4-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.67 h / -78 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: silver tetrafluoroborate / toluene / 10 h / 80 °C / Inert atmosphere; Schlenk technique

With silver tetrafluoroborate; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;
DOI:10.1021/jo401330t