(E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

Base Information

Chemical Name:(E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate
CAS No.:1357589-74-2
Molecular Formula:C₁₆H₁₉FO₃S₂
Molecular Weight:342.455
Hs Code.:

Synonyms:(E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

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Chemical Property of (E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

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Technology Process of (E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

There total 4 articles about (E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1357589-72-0
C₁₇H₂₃FO₄S₃

: 1357589-74-2
(E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

Guidance literature:: In toluene; Reflux; Inert atmosphere;
DOI:10.1021/ol203387r

Reference yield:

: 1737-16-2
1-allyl-4-fluorobenzene

: 1357589-74-2
(E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: dilauryl peroxide / ethyl acetate / 70 - 75 °C / Inert atmosphere

2: toluene / Reflux; Inert atmosphere

With dilauryl peroxide; In ethyl acetate; toluene;
DOI:10.1021/ol203387r

Reference yield:

: 1357589-51-5
ethyl 2-((ethoxycarbonothioyl)thio)-2-(methylthio)acetate

: 1357589-74-2
(E)-ethyl 4-((ethoxycarbonothioyl)thio)-5-(4-fluorophenyl)pent-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

2: dilauryl peroxide / ethyl acetate / 70 - 75 °C / Inert atmosphere

3: toluene / Reflux; Inert atmosphere

With dilauryl peroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; ethyl acetate; toluene;
DOI:10.1021/ol203387r