(2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

Base Information

Chemical Name:(2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol
CAS No.:862843-69-4
Molecular Formula:C₄₆H₆₆O₆
Molecular Weight:715.026
Hs Code.:

Synonyms:(2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

Suppliers and Price of (2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

There total 2 articles about (2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 850430-68-1
Acetic acid (2R,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-yl ester

: 862843-69-4
(2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1055/s-2004-837221

Reference yield:

: 79218-68-1,88988-46-9,93495-88-6,108869-76-7,127875-27-8,127875-34-7,129214-38-6,148968-88-1
2-O-acetyl-3,4,6-tri-O-benzyl-D-glucopyranose

: 862843-69-4
(2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / acetone / 20 °C

2: 92 percent / TMSOTf; 4 Angstroem molecular sieves / CH₂Cl₂ / 0 °C

3: 80 percent / K₂CO₃ / tetrahydrofuran; methanol / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1055/s-2004-837221

Reference yield: 80.0%

: 862843-69-4
(2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-(1-nonyl-dec-9-enyloxy)-tetrahydro-pyran-3-ol

: 850430-69-2
10-((2R,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-3-hydroxy-tetrahydro-pyran-2-yloxy)-nonadecan-2-one

Guidance literature:: With copper diacetate; oxygen; palladium dichloride; In N,N-dimethyl acetamide; at 50 ℃; under 760 Torr;
DOI:10.1055/s-2004-837221