1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

Base Information

Chemical Name:1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane
CAS No.:257890-49-6
Molecular Formula:C₄₀H₅₂N₄O₄
Molecular Weight:652.877
Hs Code.:

Synonyms:1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

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Chemical Property of 1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

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Technology Process of 1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

There total 4 articles about 1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 257890-39-4
4,10,16,22-tetraphenyl-1,7,13,19-tetraoxa-4,10,16,22-tetraaza-cyclotetracosane-3,11,15,23-tetraone

: 257890-49-6
1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

Guidance literature:: With borane-THF; In tetrahydrofuran; for 10h; Heating;
DOI:10.1016/S0040-4020(99)00892-3

Reference yield:

: 62-53-3
aniline

: 257890-49-6
1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

Guidance literature:: Multi-step reaction with 3 steps

1: 6 h / 100 °C

2: 58 percent / pyridine / toluene / 20 °C

3: 63 percent / BH₃*THF / tetrahydrofuran / 10 h / Heating

With pyridine; borane-THF; In tetrahydrofuran; toluene; 1: Substitution / 2: Cycloaddition / 3: Reduction;
DOI:10.1016/S0040-4020(99)00892-3

Reference yield:

: 75953-71-8
N,N'-diphenyl-1,5-diamino-3-oxapentane

: 257890-49-6
1,7,13,19-tetraphenyl-4,10,16,22-tetraoxa-1,7,13,19-tetraazacyclotetraeicosane

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / pyridine / toluene / 20 °C

2: 63 percent / BH₃*THF / tetrahydrofuran / 10 h / Heating

With pyridine; borane-THF; In tetrahydrofuran; toluene; 1: Cycloaddition / 2: Reduction;
DOI:10.1016/S0040-4020(99)00892-3