[(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)]

Base Information

• Chemical Name: [(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)]
• CAS No.: 933039-63-5
• Molecular Formula: C₂₈H₂₆Fe₂NO₅PS₂
• Molecular Weight: 663.318

Synonyms:[(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)]

Chemical Property of [(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)]

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Technology Process of [(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)]

There total 1 articles about [(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

[(μ-(SCH2)2N(CH2CH2CH3))Fe2(CO)6] + triphenylphosphine (603-35-0) → [(μ-SCH2N(C3H7)CH2S)Fe2(CO)5(PPh3)] (933039-63-5)

Guidance literature:

With Me₃NO*2H₂O; In dichloromethane; acetonitrile; byproducts: CO, SPPh3; (N2); std. Schlenk technique; soln. of Fe complex in MeCN was added dropwise to soln. of Me3NO*2H2O (1 equiv.) in MeCN at room temp.; soln. of PPh3 (1 equiv.) in CH2Cl2 was added during 10 min; recated for 30 min; solvent removed; chromd. (silica gel, CH2Cl2/hexane, 1/2); elem. anal.;

DOI:10.1016/j.jorganchem.2006.12.009

upstream raw materials:

triphenylphosphine

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