5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

Base Information

Chemical Name:5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide
CAS No.:150271-95-7
Molecular Formula:C₁₇H₂₃Cl₂N₅O₆
Molecular Weight:464.306
Hs Code.:

5-<N,N-bis(2-chloroethyl)amino>-N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

Synonyms:5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

Chemical Property:

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Technology Process of 5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

There total 6 articles about 5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2038-03-1
4-(2-AMINOETHYL)MORPHOLINE

: 156423-11-9
5--2,4-dinitrobenzoyl chloride

: 150271-95-7
5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

Guidance literature:: In acetone; at 0 ℃; for 0.25h;
DOI:10.1021/jm00040a009

Reference yield:

: 150272-08-5
methyl 5-chloro-2,4-dinitrobenzoate

: 150271-95-7
5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / dioxane / 3 h / 50 °C

2: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

3: LiCl / dimethylformamide / 0.01 h / 120 °C

4: 100 percent / 4 n aq. KOH / dioxane / 0.25 h / 20 °C

5: SOCl₂, DMF / 0.33 h / Heating

6: 72 percent / acetone / 0.25 h / 0 °C

With potassium hydroxide; thionyl chloride; triethylamine; N,N-dimethyl-formamide; lithium chloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00040a009

Reference yield:

: 150271-91-3
SN 24939

: 150271-95-7
5--N-<2-(4-morpholino)ethyl>-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / 0.33 h / Heating

2: 72 percent / acetone / 0.25 h / 0 °C

With thionyl chloride; N,N-dimethyl-formamide; In acetone;
DOI:10.1021/jm00040a009