N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

Base Information

Chemical Name:N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid
CAS No.:76698-50-5
Molecular Formula:C₂₈H₂₈N₂O₈
Molecular Weight:520.539
Hs Code.:

Synonyms:N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

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Chemical Property of N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

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Technology Process of N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

There total 1 articles about N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid dimethyl ester

: 76698-50-5
N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

Guidance literature:: With sodium hydroxide; In methanol; at 50 ℃; for 0.5h;

Reference yield: 83.0%

: 76698-50-5
N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

: 76698-49-2
N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic anhydride

Guidance literature:: In acetic anhydride; Ambient temperature;

Reference yield:

: 76698-50-5
N-benzyloxycarbonyl-O-benzyltyrosyliminodiacetic acid

: tyrosyl-N-(carboxymethylglycylglycylphenylalanylleucine)glycylphenylalanylleucine acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / acetic anhydride / Ambient temperature

2: 81 percent / triethylamine / ethyl acetate / Ambient temperature

3: 1.) ethyl chloroformate, N-methylmorpholine; 2.) N-methylmorpholine / 1.) DMF, 10 min; 2.) DMF, 60 min, -5 deg C; 30 min, r.t.

4: 87 percent / 1 N sodium hydroxide / methanol / 2 h / Ambient temperature

5: 79 percent / hydrogen / 5percent palladium / methanol / 760 Torr / Ambient temperature

With 4-methyl-morpholine; sodium hydroxide; hydrogen; chloroformic acid ethyl ester; triethylamine; palladium; In methanol; acetic anhydride; ethyl acetate;