2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

Base Information

Chemical Name:2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion
CAS No.:135979-33-8
Molecular Formula:C₂₆H₃₂O₃
Molecular Weight:392.538
Hs Code.:

Synonyms:2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

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Chemical Property of 2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

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Technology Process of 2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

There total 4 articles about 2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 135979-30-5
2-(3,5-di-tert-butyl-5-hydroxyphenyl)-1,4-naphthoquinone

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 135979-32-7
2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-3-methyl-1,4-naphthochinon

: 135979-33-8
2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

Guidance literature:: With dihydrogen peroxide; iron(II) sulfate; In 1,4-dioxane; at 0 - 5 ℃; for 0.25h;
DOI:10.1002/ardp.2503240806

Reference yield:

: 128-39-2
2,6-di-tert-butylphenol

: 135979-33-8
2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / dimethylsulfoxide / 12 h / Ambient temperature

2: FeSO₄*7 H₂O, 30percent H₂O₂ / dioxane / 0.25 h / 0 - 5 °C

With dihydrogen peroxide; potassium carbonate; iron(II) sulfate; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1002/ardp.2503240806

Reference yield:

: 1010-60-2
2-chloro-1,4-naphthoquinone

: 135979-33-8
2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2,3-dimethyl-1,2,3,4-tetrahydronaphthalin-1,4-dion

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / dimethylsulfoxide / 12 h / Ambient temperature

2: FeSO₄*7 H₂O, 30percent H₂O₂ / dioxane / 0.25 h / 0 - 5 °C

With dihydrogen peroxide; potassium carbonate; iron(II) sulfate; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1002/ardp.2503240806