C₅₃H₈₈O₈Si₃

Base Information

Chemical Name:C₅₃H₈₈O₈Si₃
CAS No.:214483-89-3
Molecular Formula:C₅₃H₈₈O₈Si₃
Molecular Weight:937.533
Hs Code.:

C<sub>53</sub>H<sub>88</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₅₃H₈₈O₈Si₃

Suppliers and Price of C₅₃H₈₈O₈Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₃H₈₈O₈Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₃H₈₈O₈Si₃

There total 16 articles about C₅₃H₈₈O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 214484-10-3
C₃₅H₄₈O₈Si

: 214483-89-3
C₅₃H₈₈O₈Si₃

Guidance literature:: With pyridine; dmap; for 15h;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 214484-04-5
(5S,6E)-5-methyl-2-[(1R,2E)-1-methyl-5-(benzyloxy)-2-pentenyl]-3-oxo-9-(benzyloxy)-6-nonenoic acid ethyl ester

: 214483-89-3
C₅₃H₈₈O₈Si₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: 96 percent / aq. LiCl / dimethylsulfoxide / 0.67 h / 190 °C

2.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C

3.1: CSA / benzene; methanol / 32 h

3.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

4.1: 98 percent / TFA / methanol / 0.83 h / Heating

5.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

6.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

6.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

6.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

7.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

8.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

9.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

10.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

11.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

12.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

13.1: 99 percent / pyridine; DMAP / 15 h

With pyridine; dmap; lithium hydroxide; AD-mix-α; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 440643-05-0
(3S,4S,5S,9S,10S,11S)-1,13-bis(benzyloxy)-5,9-dimethyl-3,4,10,11-tetrahydroxytridecane-7-one

: 214483-89-3
C₅₃H₈₈O₈Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: CSA / benzene; methanol / 32 h

1.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

2.1: 98 percent / TFA / methanol / 0.83 h / Heating

3.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

4.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

4.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

4.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

5.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

6.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

7.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

8.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

9.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

10.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

11.1: 99 percent / pyridine; DMAP / 15 h

With pyridine; dmap; lithium hydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9