1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

Base Information

Chemical Name:1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole
CAS No.:107450-96-4
Molecular Formula:C₃₁H₂₇N₃O₅
Molecular Weight:521.572
Hs Code.:

Synonyms:1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

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Technology Process of 1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

There total 4 articles about 1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 89174-94-7
1-phenyl-2-methyl-4-benzoyl-5-aminobenzimidazole

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 107450-96-4
1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

Guidance literature:: With sodium carbonate; In acetic acid methyl ester; benzene; at 20 ℃; for 8h;
DOI:10.1007/BF01175063

Reference yield:

: 14625-61-7
2-methyl-5-nitro-1-phenyl-1H-benzo[d]imidazole

: 107450-96-4
1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaOH / methanol / 5 h / Heating

2: 89 percent / N₂H_4.H₂O / Raney Ni / ethanol / 4 h / Heating

3: 83 percent / Na₂CO₃ / methyl acetate; benzene / 8 h / 20 °C

With sodium hydroxide; sodium carbonate; hydrazine hydrate; nickel; In methanol; ethanol; acetic acid methyl ester; benzene;
DOI:10.1007/BF01175063

Reference yield:

: 140-29-4
phenylacetonitrile

: 107450-96-4
1-phenyl-2-methyl-4-benzoyl-5-trimethoxybenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaOH / methanol / 5 h / Heating

2: 89 percent / N₂H_4.H₂O / Raney Ni / ethanol / 4 h / Heating

3: 83 percent / Na₂CO₃ / methyl acetate; benzene / 8 h / 20 °C

With sodium hydroxide; sodium carbonate; hydrazine hydrate; nickel; In methanol; ethanol; acetic acid methyl ester; benzene;
DOI:10.1007/BF01175063