methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

Base Information

Chemical Name:methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate
CAS No.:139932-41-5
Molecular Formula:C₁₄H₂₁BrO₂Si
Molecular Weight:329.309
Hs Code.:

Synonyms:methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

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Chemical Property of methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

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Technology Process of methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

There total 4 articles about methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114671-13-5
methyl 3-(4'-methyl)phenyl-3-trimethylsilylpropanoate

: 139932-41-5
methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; Irradiation;
DOI:10.1016/S0040-4039(01)83873-9

Reference yield:

: 1866-39-3,940-61-4
trans-p-methylcinnamic acid

: 139932-41-5
methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: Mg, N,N-dimethyl ethylene urea (DMEU) / tetrahydrofuran / 55 - 60 °C

3: N-bromosuccinimide / CCl₄ / Irradiation

With N,N-dimethyl ethylene urea; N-Bromosuccinimide; thionyl chloride; magnesium; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4039(01)83873-9

Reference yield:

: 20754-20-5
3-p-tolyl-acrylic acid methyl ester

: 139932-41-5
methyl 3-<(4'-bromomethyl)phenyl>-3-trimethylsilylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Mg, N,N-dimethyl ethylene urea (DMEU) / tetrahydrofuran / 55 - 60 °C

2: N-bromosuccinimide / CCl₄ / Irradiation

With N,N-dimethyl ethylene urea; N-Bromosuccinimide; magnesium; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4039(01)83873-9