N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

Base Information

Chemical Name:N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin
CAS No.:161885-41-2
Molecular Formula:C₂₃H₃₀N₂O₅
Molecular Weight:414.502
Hs Code.:

Synonyms:N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

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Chemical Property of N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

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Technology Process of N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

There total 3 articles about N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 161885-40-1
N-<3-propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

: 161885-41-2
N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;
DOI:10.1016/S0968-0896(98)00166-7

Reference yield:

: 39217-14-6
N-(3,4-dimethoxyphenyl)-N-benzylamine

: 161885-41-2
N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / 1.5 h / 100 °C

2: 93 percent / hydrogene / Pd/C / methanol / Ambient temperature

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/S0968-0896(98)00166-7

Reference yield:

: 85175-65-1
7,8-dimethoxy-3-(3-chloropropyl)-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

: 161885-41-2
N-<3-N-(3,4-dimethoxyphenyl)propylamino>-7,8-dimethoxy-2,3,4,5-tetrahydro-2-oxo-1H-3-benzazepin

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / 1.5 h / 100 °C

2: 93 percent / hydrogene / Pd/C / methanol / Ambient temperature

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/S0968-0896(98)00166-7