N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine

Base Information

Chemical Name:N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine
CAS No.:1592078-30-2
Molecular Formula:C₂₆H₂₈N₂O₂Si
Molecular Weight:428.606
Hs Code.:

Synonyms:N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine

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Chemical Property of N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine

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Technology Process of N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine

There total 2 articles about N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1352010-04-8
N-(diphenylmethylene)-2-trimethylsilylethynamine

: 917-54-4
methyllithium

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1592078-30-2
N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine

Guidance literature:: N-(diphenylmethylene)-2-trimethylsilylethynamine; methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.333333h; Inert atmosphere;

1-bromomethyl-4-nitro-benzene; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol500749h

Reference yield:

: 53210-13-2
copper(I) (trimethylsilyl)acetylide

: 1592078-30-2
N-(1,1-diphenylethyl)-3-(4-nitrophenyl)-2-(trimethylsilyl)prop-1-en-1-imine

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxygen; 1,2-dimethyl-1H-imidazole / acetonitrile / 12 h / 20 °C

2.1: tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C / Inert atmosphere

With 1,2-dimethyl-1H-imidazole; oxygen; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/ol500749h