Technology Process of C27H33N9O5
There total 8 articles about C27H33N9O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H37N9O5;
With
water; trifluoroacetic acid;
palladium 10% on activated carbon;
In
ethanol;
at 20 ℃;
for 1h;
In
methanol;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / Reflux
2.1: N-ethyl-N,N-diisopropylamine; bis(trichloromethyl) carbonate / dichloromethane / 1.5 h / 0 - 20 °C
2.2: 0 - 20 °C
3.1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr
4.1: trifluoroacetic acid; water / palladium 10% on activated carbon / ethanol / 1 h / 20 °C
4.2: basic resin / 1 h / 20 °C
With
bis(trichloromethyl) carbonate; water; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium 10% on activated carbon;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / Reflux
2.1: N-ethyl-N,N-diisopropylamine; bis(trichloromethyl) carbonate / dichloromethane / 1.5 h / 0 - 20 °C
2.2: 0 - 20 °C
3.1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr
4.1: trifluoroacetic acid; water / palladium 10% on activated carbon / ethanol / 1 h / 20 °C
4.2: basic resin / 1 h / 20 °C
With
bis(trichloromethyl) carbonate; water; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium 10% on activated carbon;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;