1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

Base Information

Chemical Name:1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene
CAS No.:549507-68-8
Molecular Formula:C₅₁H₆₄N₈O₁₀
Molecular Weight:949.117
Hs Code.:

1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

Synonyms:1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

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Chemical Property of 1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

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Technology Process of 1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

There total 9 articles about 1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 549507-67-7
1-[(3-(N,N-bis(6-(2,2'-bipyridyl)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

: 549507-68-8
1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 20h;
DOI:10.1002/chem.200390003

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 549507-68-8
1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 23 percent / CH₂Cl₂ / 21 h

2: 97 percent / DCC; HOBt / CH₂Cl₂ / 14 h / 20 °C

3: 69 percent / m-chlroperbenzoic acid / CHCl₃ / 20 h / 20 °C

With benzotriazol-1-ol; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In dichloromethane; chloroform;
DOI:10.1002/chem.200390003

Reference yield:

: 82740-65-6
6-(chloromethyl)-2,2’-bipyridine

: 549507-68-8
1-[(3-(N,N-bis(6-(2,2'-bipyridyl-1,1'-dioxide)methyl)carbamoyl)propanoyl)aminomethyl]-3,5-bis[N-((tert-butoxy)carbonyl)aminomethyl]-2,4,6-triethylbenzene

Guidance literature:: Multi-step reaction with 6 steps

1: 72 percent / K₂CO₃ / dimethylformamide / 6 h / 100 °C

2: 95 percent / aq. H₂SO₄ / 2 h / 120 °C

3: 97 percent / DCC; HOBt / CH₂Cl₂ / 6.5 h / 0 - 20 °C

4: 95 percent / aq. KOH / methanol / 5 h / 90 °C

5: 97 percent / DCC; HOBt / CH₂Cl₂ / 14 h / 20 °C

6: 69 percent / m-chlroperbenzoic acid / CHCl₃ / 20 h / 20 °C

With potassium hydroxide; sulfuric acid; potassium carbonate; benzotriazol-1-ol; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200390003