3-oxabicyclo[3.2.1]octan-8-one

Base Information

• Chemical Name: 3-oxabicyclo[3.2.1]octan-8-one
• CAS No.: 625099-16-3
• Molecular Formula: C₇H₁₀O₂
• Molecular Weight: 126.155

Synonyms:3-oxabicyclo[3.2.1]octan-8-one

Chemical Property of 3-oxabicyclo[3.2.1]octan-8-one

Chemical Property:

• Boiling Point: 214.7±15.0 °C(Predicted)
• Density: 1.141±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

3-Oxabicyclo[3.2.1]octan-8-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 3-Oxabicyclo[3.2.1]octan-8-one is derived from exo-?2,?3-?Epoxynorbornane (E891988), which is a cytotoxic epoxide compound which also may act as a mutagen.

Technology Process of 3-oxabicyclo[3.2.1]octan-8-one

There total 7 articles about 3-oxabicyclo[3.2.1]octan-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H14O3 (625099-19-6) → 3-oxabicyclo[3.2.1]octan-8-one (625099-16-3)

Guidance literature:

With hydrogenchloride; water; at 20 ℃;

Reference yield:

C9H16O4 (625099-17-4) → 3-oxabicyclo[3.2.1]octan-8-one (625099-16-3)

Guidance literature:

Multi-step reaction with 3 steps

1: silver(l) oxide / potassium iodide / dichloromethane / 72 h / 20 °C

2: potassium carbonate / methanol / 20 °C

3: hydrogenchloride; water / 20 °C

With hydrogenchloride; water; potassium carbonate; silver(l) oxide; potassium iodide; In methanol; dichloromethane;

Reference yield:

anti-bicyclo<2.2.1>hept-2-en-7-ol (53783-87-2) → 3-oxabicyclo[3.2.1]octan-8-one (625099-16-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

1.2: 0.5 h / -78 - 20 °C

2.1: toluene-4-sulfonic acid / benzene / 4 h / Reflux

3.1: ozone / dichloromethane; methanol / -78 °C

3.2: -78 - 0 °C

4.1: silver(l) oxide / potassium iodide / dichloromethane / 72 h / 20 °C

5.1: potassium carbonate / methanol / 20 °C

6.1: hydrogenchloride; water / 20 °C

With hydrogenchloride; oxalyl dichloride; water; potassium carbonate; toluene-4-sulfonic acid; ozone; dimethyl sulfoxide; silver(l) oxide; potassium iodide; In methanol; dichloromethane; benzene;

upstream raw materials:

C₉H₁₆O₄

C₁₆H₂₂O₆S

anti-bicyclo<2.2.1>hept-2-en-7-ol

7-norbornenone

Downstream raw materials:

C₁₈H₂₁NO₅

C₁₈H₂₃NO₅

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