(Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide

Base Information

• Chemical Name: (Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide
• CAS No.: 1194509-21-1
• Molecular Formula: C₁₅H₁₈INO₃
• Molecular Weight: 387.217
• Mol file: 1194509-21-1.mol

Synonyms:(Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide

Chemical Property of (Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide

There total 1 articles about (Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

propynoic acid (2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)amide (1194509-18-6) → (Z)-N-(2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)-3-iodoacrylamide (1194509-21-1)

Guidance literature:

propynoic acid (2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)amide; With aluminum (III) chloride; sodium iodide; In dichloromethane; tert-butyl alcohol; at 20 ℃; for 18h; Inert atmosphere;

With water; In dichloromethane; tert-butyl alcohol; stereoselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2009.08.032

upstream raw materials:

propynoic acid (2,2-dimethyl-4-phenyl-1,3-dioxan-5-yl)amide