(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

Base Information

Chemical Name:(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal
CAS No.:1336874-16-8
Molecular Formula:C₁₇H₁₆O₃
Molecular Weight:268.312
Hs Code.:

Synonyms:(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

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Chemical Property of (+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

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Technology Process of (+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

There total 5 articles about (+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1336874-14-6
(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutan-1-ol

: 1336874-16-8
(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm200782y

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 1336874-16-8
(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

Guidance literature:: Multi-step reaction with 5 steps

1.1: piperidine; acetic acid / toluene / 24 h / 150 °C

2.1: copper(l) chloride / diethyl ether / -78 - 20 °C / Inert atmosphere

3.1: potassium hydroxide / methanol; water / 24 h / 20 °C

3.2: 0 °C / pH 2

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 4.5 h / 0 - 20 °C

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

With piperidine; lithium aluminium tetrahydride; sulfur trioxide pyridine complex; acetic acid; dimethyl sulfoxide; triethylamine; copper(l) chloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; 1.1: Knoevenagel condensation;
DOI:10.1021/jm200782y

Reference yield:

: 5458-69-5
diethyl 2-[(1,3-benzodioxol-5-yl)methylideene]-malonate

: 1336874-16-8
(+/-)-3-(benzo[d][1,3]dioxol-5-yl)-4-phenylbutanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) chloride / diethyl ether / -78 - 20 °C / Inert atmosphere

2.1: potassium hydroxide / methanol; water / 24 h / 20 °C

2.2: 0 °C / pH 2

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 4.5 h / 0 - 20 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

With lithium aluminium tetrahydride; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; copper(l) chloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/jm200782y