1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

Base Information

Chemical Name:1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine
CAS No.:1449738-06-0
Molecular Formula:C₂₃H₃₄N₂
Molecular Weight:338.536
Hs Code.:

1-(3-cyclopentyl-1-tricyclo[3.3.1.1<sup>3,7</sup>] decyl)-N<sup>1</sup>-phenyl-1,2-ethanediamine

Synonyms:1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

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Chemical Property of 1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

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Technology Process of 1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

There total 3 articles about 1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1449650-88-7
3-cyclopentyl-α-phenylamino-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile

: 1449738-06-0
1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

Guidance literature:: 3-cyclopentyl-α-phenylamino-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile; With borane-THF; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere; Reflux;

With water; In tetrahydrofuran; at 0 ℃;

With hydrogenchloride; In water; for 4h; Reflux;
DOI:10.1039/c3md00081h

Reference yield:

: 160013-51-4
3-cyclopentyl-1-tricyclo<3.3.1.1.^3,7>decanecarboxylic acid

: 1449738-06-0
1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C

1.2: 0 °C

2.1: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

3.1: acetonitrile / 45 h / 20 °C / Inert atmosphere

4.1: borane-THF / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Reflux

4.2: 0 °C

4.3: 4 h / Reflux

With lithium aluminium tetrahydride; borane-THF; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile; 3.1: |Strecker Aminoacid Synthesis;
DOI:10.1039/c3md00081h

Reference yield:

: 3-cyclopentyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

: 1449738-06-0
1-(3-cyclopentyl-1-tricyclo[3.3.1.1^3,7] decyl)-N¹-phenyl-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.1: acetonitrile / 45 h / 20 °C / Inert atmosphere

3.1: borane-THF / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Reflux

3.2: 0 °C

3.3: 4 h / Reflux

With borane-THF; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile; 2.1: |Strecker Aminoacid Synthesis;
DOI:10.1039/c3md00081h